Haloalkanes and Haloarenes - Reaction with Metals

  • Haloalkanes and haloarenes undergo various reactions with metals.
  • These reactions involve the displacement of the halogen atom by the metal atom.
  • Here, we will discuss the reaction of haloalkanes and haloarenes with different metals.

Reaction with Sodium (Na)

  • Haloalkanes react with sodium to form an alkane and sodium halide.
  • For example, 2-chloropropane reacts with sodium to form propane and sodium chloride: CH3CHClCH3 + 2Na → CH3CH2CH3 + 2NaCl
  • Similarly, haloarenes also react with sodium to form an arene and sodium halide.

Reaction with Magnesium (Mg)

  • Haloalkanes react with magnesium in the presence of anhydrous ether (diethyl ether) to form Grignard reagents.
  • Grignard reagents are important intermediates in organic synthesis.
  • For example, ethyl bromide reacts with magnesium to form ethylmagnesium bromide: C2H5Br + Mg → C2H5MgBr
  • Grignard reagents can further react with carbonyl compounds, forming alcohols or carboxylic acids.

Reaction with Zinc (Zn)

  • Haloalkanes react with zinc in the presence of dry ether to form organozinc compounds.
  • These reactions are known as the Negishi coupling reactions.
  • For example, bromobenzene reacts with zinc to form phenylzinc bromide: C6H5Br + Zn → C6H5ZnBr
  • Organozinc compounds can further react with various electrophiles, creating different organic products.

Reaction with Iron (Fe)

  • Haloalkanes react with iron in the presence of ether to form alkyl iron complexes.
  • These complexes are used as reagents in organic synthesis.
  • For example, 1-bromobutane reacts with iron to form tert-butyliron(II) chloride: CH3CH2CH2CH2Br + Fe → (CH3)3CFeCl
  • Alkyl iron complexes can undergo various reactions, such as oxidative addition or substitution.

Reaction with Silver (Ag)

  • Haloalkanes react with silver in the presence of ammonia to form a complex called silver halide complex.
  • This complex is soluble in ammonia.
  • For example, bromoethane reacts with silver in the presence of ammonia to form silver bromide complex: C2H5Br + Ag + 2NH3 → [Ag(NH3)2]Br
  • This reaction is used in the analytical determination of halides.
  1. Reaction with Copper (Cu)
  • Haloalkanes and haloarenes do not react directly with copper.
  • However, they can react with copper in the presence of a catalyst to form copper(I) species.
  • For example, bromoethane reacts with copper in the presence of a reducing agent to form ethyl copper: C2H5Br + 2Cu + 2Li → C2H5Cu + 2LiBr
  • Copper(I) species can further react with various electrophiles, resulting in the formation of different organic products.
  1. Reaction with Lithium (Li)
  • Haloalkanes react with lithium in the presence of anhydrous ether (diethyl ether) to form organolithium compounds.
  • Organolithium compounds are strong bases and nucleophiles.
  • For example, 1-bromopropane reacts with lithium to form n-propyllithium: CH3CH2CH2Br + 2Li → CH3CH2CH2Li + LiBr
  • Organolithium compounds can undergo various reactions, such as nucleophilic substitution or addition.
  1. Reaction with Potassium (K)
  • Haloalkanes react with potassium to form organopotassium compounds.
  • Organopotassium compounds are strong bases and nucleophiles, similar to organolithium compounds.
  • For example, 1-iodobutane reacts with potassium to form n-butyllithium: CH3CH2CH2CH2I + 2K → CH3CH2CH2CH2K + KI
  • Organopotassium compounds can also undergo nucleophilic substitution or addition reactions.
  1. Reaction with Aluminum (Al)
  • Haloalkanes react with aluminum in the presence of ether to form alkyl aluminum compounds.
  • These compounds are known as alkylaluminums or aluminum alkyls.
  • For example, ethyl bromide reacts with aluminum to form triethylaluminum: C2H5Br + Al → (C2H5)3Al
  • Alkylaluminums can further react with various electrophiles, yielding diverse organic products.
  1. Reaction with Gold (Au)
  • Haloalkanes do not react directly with gold.
  • However, they can react with gold in the presence of a catalyst to form organogold complexes.
  • For example, chloroethane reacts with gold in the presence of a silver catalyst to form ethyl gold(I) chloride: C2H5Cl + Au + Ag → C2H5AuCl + AgCl
  • Organogold complexes can undergo various reactions, including substitution or insertion processes.
  1. Reaction with Platinum (Pt)
  • Haloalkanes and haloarenes do not react directly with platinum.
  • However, they can react with platinum in the presence of a catalyst to form organoplatinum complexes.
  • For example, bromobenzene reacts with platinum in the presence of tin(II) chloride to form phenylplatinum(II) chloride: C6H5Br + Pt + SnCl2 → C6H5PtCl + SnCl4
  • Organoplatinum complexes can participate in a range of reactions, such as oxidative addition, migratory insertion, or ligand exchange.
  1. Reaction with Mercury (Hg)
  • Haloalkanes react with mercury in the presence of an acid catalyst to form organomercury compounds.
  • Organomercury compounds are less common due to their high toxicity.
  • For example, bromoethane reacts with mercury in the presence of hydrochloric acid to form ethylmercury chloride: C2H5Br + Hg + HCl → C2H5HgCl + HBr
  • Organomercury compounds can undergo various reactions, but their use is restricted due to their adverse effects on health and the environment.
  1. Reaction with Nickel (Ni)
  • Haloalkanes and haloarenes do not react directly with nickel.
  • But they can react with nickel in the presence of a catalyst to form organonickel complexes.
  • For example, bromobenzene reacts with nickel in the presence of triethylamine to form phenylnickel(II) bromide: C6H5Br + Ni + (C2H5)3N → C6H5NiBr + (C2H5)3NHBr
  • Organonickel complexes can participate in various reactions, such as oxidative addition, reductive elimination, or migratory insertion.
  1. Reaction with Palladium (Pd)
  • Haloalkanes and haloarenes do not react directly with palladium.
  • However, they can react with palladium in the presence of a catalyst to form organopalladium complexes.
  • For example, 2-bromopropane reacts with palladium in the presence of triphenylphosphine to form isopropylpalladium bromide: (CH3)2CHBr + Pd + PPh3 → (CH3)2CHPdBr + PPh3Br
  • Organopalladium complexes can participate in various reactions, including oxidative addition, reductive elimination, or cross-coupling reactions.
  1. Summary
  • Haloalkanes and haloarenes can undergo different reactions with metals.
  • These reactions involve the displacement of the halogen atom by the metal atom.
  • Reactions with metals include the formation of alkyl or aryl metal compounds.
  • Some important metal reactions include those with sodium, magnesium, zinc, iron, copper, lithium, potassium, aluminum, gold, platinum, mercury, nickel, and palladium.
  1. Reaction with Sodium (Na)
  • Haloalkanes react with sodium to form an alkane and sodium halide.
  • Example: 2-Chloropropane + Sodium → Propane + Sodium Chloride.
  1. Reaction with Magnesium (Mg)
  • Haloalkanes react with magnesium in the presence of anhydrous ether.
  • This forms Grignard reagents, which are important intermediates in organic synthesis.
  • Example: Ethyl Bromide + Magnesium → Ethylmagnesium Bromide.
  1. Reaction with Zinc (Zn)
  • Haloalkanes react with zinc in the presence of dry ether to form organozinc compounds.
  • This reaction is called the Negishi coupling reaction.
  • Example: Bromobenzene + Zinc → Phenylzinc Bromide.
  1. Reaction with Iron (Fe)
  • Haloalkanes react with iron in the presence of ether to form alkyl iron complexes.
  • These complexes are used as reagents in organic synthesis.
  • Example: 1-Bromobutane + Iron → tert-Butyliron(II) Chloride.
  1. Reaction with Silver (Ag)
  • Haloalkanes react with silver in the presence of ammonia to form a soluble silver halide complex.
  • Example: Bromoethane + Silver + Ammonia → [Ag(NH3)2]Br.
  1. Reaction with Copper (Cu)
  • Haloalkanes and haloarenes can react with copper in the presence of a catalyst.
  • This leads to the formation of copper(I) species, which can react with electrophiles.
  • Example: Bromoethane + Copper + Reducing Agent → Ethyl Copper.
  1. Reaction with Lithium (Li)
  • Haloalkanes react with lithium in the presence of anhydrous ether to form organolithium compounds.
  • Organolithium compounds are strong bases and nucleophiles.
  • Example: 1-Bromopropane + Lithium → n-Propylithium.
  1. Reaction with Potassium (K)
  • Haloalkanes react with potassium to form organopotassium compounds.
  • These compounds are strong bases and nucleophiles.
  • Example: 1-Iodobutane + Potassium → n-Butyllithium.
  1. Reaction with Aluminum (Al)
  • Haloalkanes react with aluminum in the presence of ether to form alkyl aluminum compounds.
  • Example: Ethyl Bromide + Aluminum → Triethylaluminum.
  1. Reaction with Gold (Au)
  • Haloalkanes can react with gold in the presence of a catalyst to form organogold complexes.
  • Example: Chloroethane + Gold + Silver catalyst → Ethyl Gold(I) Chloride.