Alcohols - Solved Examples

  • Example 1:
    • Write the IUPAC name of the following compound:
      • CH3-CH2-CH2-OH
    • Solution:
      • The IUPAC name of the given compound is “propanol”.
  • Example 2:
    • Classify the following compounds as primary, secondary, or tertiary alcohols:
      • CH3-CH2-OH
      • (CH3)2CH-OH
      • (CH3)3C-OH
    • Solution:
      • CH3-CH2-OH is a primary alcohol.
      • (CH3)2CH-OH is a secondary alcohol.
      • (CH3)3C-OH is a tertiary alcohol.
  • Example 3:
    • Write the structural formula for the following compounds:
      • Ethanol
      • Isopropanol
    • Solution:
      • Ethanol: CH3-CH2-OH
      • Isopropanol: (CH3)2CH-OH
  • Example 4:
    • Classify the following alcohols as primary, secondary, or tertiary:
      • 2-butanol
      • Cyclohexanol
    • Solution:
      • 2-butanol is a secondary alcohol.
      • Cyclohexanol is a tertiary alcohol.
  • Example 5:
    • Convert the following alcohol into an alkene:
      • CH3-CH2-CH2-OH
    • Solution:
      • By eliminating one molecule of water, CH3-CH=CH2 can be obtained.

Alcohols - Solved Examples

  • Example 6:
    • Write the balanced chemical equation for the oxidation of a primary alcohol to an aldehyde.
    • Solution:
      • CH3-CH2-OH + [O] → CH3-CHO + H2O
  • Example 7:
    • Write the balanced chemical equation for the oxidation of a primary alcohol to a carboxylic acid.
    • Solution:
      • CH3-CH2-OH + 2[O] → CH3-COOH + H2O
  • Example 8:
    • Write the balanced chemical equation for the oxidation of a secondary alcohol to a ketone.
    • Solution:
      • (CH3)2CH-OH + [O] → (CH3)2C=O + H2O
  • Example 9:
    • Write the balanced chemical equation for the dehydration of an alcohol to form an alkene.
    • Solution:
      • CH3-CH2-OH → CH2=CH2 + H2O
  • Example 10:
    • Name the following compound:
      • CH3-CH2-CH2-CHO
    • Solution:
      • The IUPAC name of the given compound is “butanal”.

Ethers - Introduction

  • Definition:
    • Ethers are organic compounds that have an oxygen atom bonded to two alkyl or aryl groups.
  • General Formula:
    • R-O-R'
  • Physical Properties:
    • Ethers have a sweet or fruity odor.
    • They are less dense than water.
    • They have low boiling points compared to alcohols.
  • Nomenclature:
    • Ethers are named by identifying the two alkyl or aryl groups bonded to the oxygen atom and adding the suffix “-ether”.

Ethers - Preparation Methods

  • Preparation Method 1: Williamson Ether Synthesis
    • In this method, an alkyl halide reacts with an alkoxide ion to form an ether.
    • R-X + R’-O- → R-O-R’ + X-
  • Preparation Method 2: Dehydration of Alcohols
    • When alcohols are heated with a strong acid catalyst, they undergo dehydration to form ethers.
    • 2R-OH → R-O-R’ + H2O
  • Preparation Method 3: Alkoxymercuration-Demercuration Reaction
    • In this method, an alkene reacts with mercuric acetate and an alcohol to form an ether.
    • RCH=CH2 + R’-OH + Hg(OAc)2 → R-O-R’ + Hg(OAc)OH

Ethers - Examples and Uses

  • Example: Ethyl Ether
    • Molecular Formula: C2H5-O-C2H5
    • Common Name: Diethyl Ether
    • Uses:
      • It is used as a general anesthetic.
      • It is used as a solvent in organic synthesis.
      • It is used as a starting material for the production of other chemicals.
  • Example: Methyl Tert-Butyl Ether (MTBE)
    • Molecular Formula: (CH3)3C-O-CH3
    • Uses:
      • It is used as an octane booster in gasoline.
      • It is used as a solvent for paints, varnishes, and adhesives.
  • Example: Dimethyl Ether (DME)
    • Molecular Formula: CH3-O-CH3
    • Uses:
      • It is used as a propellant in aerosol products.
      • It is used as a clean-burning alternative fuel for diesel engines.

Epoxides - Introduction

  • Definition:
    • Epoxides, also known as oxiranes, are three-membered cyclic ethers.
  • Structure:
    • Epoxides have a strained ring structure with an oxygen atom and two carbon atoms.
  • Physical Properties:
    • Epoxides are highly reactive due to the angle strain in the three-membered ring.
    • They have higher boiling points compared to ethers.
  • Nomenclature:
    • Epoxides are named by identifying the two alkyl or aryl groups attached to the oxygen atom and adding the suffix “-epoxide”.
  • Example: Ethylene Oxide
    • Molecular Formula: C2H4O
    • Uses:
      • It is used as a sterilizing agent for medical instruments.
      • It is used in the production of various chemicals, including detergents and solvents.

Epoxides - Preparation Methods

  • Preparation Method 1: Acid-Catalyzed Epoxidation
    • In this method, alkenes react with a peroxy acid, such as peracetic acid, to form epoxides.
    • CH2=CH2 + CH3CO3H → CH2OCH2 + CH3COOH
  • Preparation Method 2: Base-Catalyzed Epoxidation
    • In this method, alkenes react with a peroxide in the presence of a base, such as sodium hydroxide, to form epoxides.
    • CH2=CH2 + H2O2 + NaOH → CH2OCH2 + NaOH2
  • Preparation Method 3: Oxirane Ring Expansion
    • In this method, cyclic ethers are treated with a strong acid or base to form epoxides.
    • CH3-CH2-OCH2-CH3 + HBr → CH3-CHOH-CH2-Br

Epoxides - Reactions

  • Ring Opening Reactions:
    • Epoxides can undergo ring-opening reactions with nucleophiles, such as water or alcohol, to form diols.
    • R-O-CH2-R + Nu- → R-OH-CH2-R-Nu
  • Acidic Cleavage Reactions:
    • Epoxides can be cleaved in the presence of a strong acid to form two carbonyl compounds.
    • R-O-CH2-R’ + H3O+ → R-C(O)H + R’-C(O)H
  • Oxidation Reactions:
    • Epoxides can be oxidized with peracids or mCPBA to form vicinal diols.
    • R-O-CH2-R’ + RCO3H → R-OH-CH(OH)-R’ + RCO2H

Summary

  • Alcohols:
    • Primary alcohols can be oxidized to aldehydes or carboxylic acids.
    • Secondary alcohols can be oxidized to ketones.
    • Alcohols can be dehydrated to form alkenes.
  • Ethers:
    • Ethers are named by identifying the two alkyl or aryl groups bonded to the oxygen atom.
    • Ethers can be prepared by Williamson Ether Synthesis, dehydration of alcohols, or alkoxymercuration-demercuration reaction.
  • Epoxides:
    • Epoxides are three-membered cyclic ethers.
    • Epoxides can be prepared by acid-catalyzed or base-catalyzed epoxidation, or oxirane ring expansion.
  • Reactions:
    • Alcohols, ethers, and epoxides can undergo various reactions such as oxidation, ring opening, and cleavage reactions.

Practice Questions

  • Identify the type of alcohol in each of the following compounds:
    • CH3-CH2-CH2-OH
    • (CH3)2CHOH
    • (CH3)3COH
  • Name the following compounds:
    • CH3-O-CH3
    • C2H5-OC2H5
    • CH3-CH2-O-C2H5
  • Write the balanced chemical equations for the following reactions:
    • Oxidation of ethanol to form ethanoic acid.
    • Dehydration of 1-butanol to form butene.
  • Classify the following compounds as ethers or epoxides:
    • CH3-CH2-O-CH2-CH3
    • C4H8O
  • Predict the product of the following reaction:
    • CH2=CH2 + H2SO4 → ?

(End of Slides 11-20)

Ethers - Physical properties

  • Ethers have a sweet or fruity odor.
  • They are less dense than water.
  • Ethers have low boiling points compared to alcohols.
  • They are generally liquid at room temperature.
  • Ethers are highly flammable.

Ethers - Reactions

  • Ethers undergo substitution reactions with halogens in the presence of a Lewis acid catalyst.
  • They can be cleaved by strong acids to form two alkyl halides.
  • Ethers can be used as solvents in organic reactions.
  • They can react with strong bases to form alcohol and alkoxide ions.
  • Ethers can participate in nucleophilic addition reactions.

Ethers - Examples and Uses

  • Example: Ethyl Ether
    • Molecular Formula: C2H5-O-C2H5
    • Common Name: Diethyl Ether
    • Uses:
      • It is used as a general anesthetic.
      • It is used as a solvent in organic synthesis.
      • It is used as a starting material for the production of other chemicals.
  • Example: Methyl Tert-Butyl Ether (MTBE)
    • Molecular Formula: (CH3)3C-O-CH3
    • Uses:
      • It is used as an octane booster in gasoline.
      • It is used as a solvent for paints, varnishes, and adhesives.
  • Example: Dimethyl Ether (DME)
    • Molecular Formula: CH3-O-CH3
    • Uses:
      • It is used as a propellant in aerosol products.
      • It is used as a clean-burning alternative fuel for diesel engines.

Ethers - Williamson Ether Synthesis

  • In Williamson Ether Synthesis, an alkyl halide reacts with an alkoxide ion to form an ether.
  • The reaction is usually carried out in the presence of a strong base, such as sodium or potassium hydroxide.
  • The alkyl halide is the electrophile and the alkoxide ion is the nucleophile in the reaction.
  • The reaction proceeds through an SN2 mechanism.

Ethers - Dehydration of Alcohols

  • When alcohols are heated with a strong acid catalyst, they undergo dehydration to form ethers.
  • The acid catalyst, such as concentrated sulfuric acid, protonates the hydroxyl group of the alcohol, making it a better leaving group.
  • The protonated alcohol then loses a water molecule, resulting in the formation of an alkene.
  • The alkene can further react with another alcohol molecule to form an ether.

Epoxides - Introduction

  • Definition:
    • Epoxides, also known as oxiranes, are three-membered cyclic ethers.
  • Structure:
    • Epoxides have a strained ring structure with an oxygen atom and two carbon atoms.
  • Physical Properties:
    • Epoxides are highly reactive due to the angle strain in the three-membered ring.
    • They have higher boiling points compared to ethers.
  • Nomenclature:
    • Epoxides are named by identifying the two alkyl or aryl groups attached to the oxygen atom and adding the suffix “-epoxide”.

Epoxides - Preparation Methods

  • Preparation Method 1: Acid-Catalyzed Epoxidation
    • In this method, alkenes react with a peroxy acid, such as peracetic acid, to form epoxides.
    • The reaction proceeds through an electrophilic addition mechanism.
  • Preparation Method 2: Base-Catalyzed Epoxidation
    • In this method, alkenes react with a peroxide in the presence of a base, such as sodium hydroxide, to form epoxides.
    • The reaction proceeds through a nucleophilic addition mechanism.
  • Preparation Method 3: Oxirane Ring Expansion
    • In this method, cyclic ethers are treated with a strong acid or base to form epoxides.
    • The reaction proceeds by breaking a carbon-oxygen bond and forming a carbon-carbon bond.

Epoxides - Reactions

  • Ring Opening Reactions:
    • Epoxides can undergo ring-opening reactions with nucleophiles, such as water or alcohol, to form diols.
    • The nucleophile attacks one of the carbon atoms in the epoxide ring, resulting in the formation of an alcohol.
    • The reaction can proceed through either an SN2 or SN1 mechanism, depending on the nucleophile and reaction conditions.
  • Acidic Cleavage Reactions:
    • Epoxides can be cleaved in the presence of a strong acid to form two carbonyl compounds.
    • The acid protonates one of the oxygen atoms in the epoxide ring, making it a better leaving group.
    • The protonated epoxide undergoes nucleophilic attack by water, resulting in the formation of two carbonyl compounds.
  • Oxidation Reactions:
    • Epoxides can be oxidized with peracids or mCPBA (meta-chloroperoxybenzoic acid) to form vicinal diols.
    • The oxygen in the epoxide ring is oxidized to a hydroxyl group, resulting in the formation of a diol.